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首页 确定流体缺失的固相线温度在活塞气缸实验的一种新方法 毕业论文外文翻译

确定流体缺失的固相线温度在活塞气缸实验的一种新方法 毕业论文外文翻译.doc

确定流体缺失的固相线温度在活塞气缸实验的一种新方法 毕业论文外…

ma永健 2017-12-22 评分 0 浏览量 0 0 0 0 暂无简介 简介 举报

简介:本文档为《确定流体缺失的固相线温度在活塞气缸实验的一种新方法 毕业论文外文翻译doc》,可适用于战略管理领域,主题内容包含确定流体缺失的固相线温度在活塞气缸实验的一种新方法毕业论文外文翻译关注豆丁网你懂的核准通过归档资料。未经允许请勿外传~外文译文确定流体缺失的固相线温符等。

确定流体缺失的固相线温度在活塞气缸实验的一种新方法毕业论文外文翻译关注豆丁网你懂的核准通过归档资料。未经允许请勿外传~外文译文确定流体缺失的固相线温度在活塞气缸实验的一种新方法摘要我们描述了一种新的活塞气缸用于确定流体缺失的地质材料的固相线的方法。样品加热增量不到一小时的期间为千巴的压力。测量油压融化的影响虽小但检测和压力时间数据的解释产生一个准确的斜线。该技术成功地再现了氯化锂的固相线。为OllodeSapo泥质片麻岩的结果是比以前使用的更传统的技术获得。简介在地球的地幔和地壳岩浆源识别促进实验岩石学的结果。PT深部原岩的固相线的位置以了解岩浆代的过程是至关重要的。潜在的地壳源材料如角闪岩和泥质岩固相线已经确定实验(例如年威利辛格和年约翰内斯皮托杜丝帕蒂诺和比尔德年年帕蒂诺杜丝和哈里斯Vielzeuf和年克莱门斯年Vielzeuf及Montel)。这些结果表明在矿物组合的变化或涉及在熔融反应(例如云母和长石)的矿物的固溶体的组合物可以产生强大的固相线温度的影响。因此为了正确地鉴定浆生产过程中在特定环境中它是必不可少的以确定特定的地壳原岩的固相线曲线。然而由于工作繁重需要许多费时的实验熔体的存在或不存在是由观察的扫描型电子显微镜(SEM)图像的运行产品。下面描述的技术可用于确定通过直接观察的活塞气缸装置中的油压的影响熔融的固相线曲线在PT空间的位置。这些影响是非常小的但可检测到的增量加热所产生的压力时间曲线(Pt)的检查。基本原理活塞缸实验我们已经注意到在的温度变化有一个可衡量的影响压力。这是一个实验期间观察到的第一分钟时温度上升配有温度控制器。测得的压力对时间作图时获得相应的斜坡。因此在加热过程中在测得的压时间曲线的斜率的压实可以被检测到的胶囊型容器和力变化影响的压力或样品日本。在胶囊内的熔化的样品将产生一个可能被检测到的压力如果非常精确地测量和数据被连续拍摄的压实效果。应用这种方法我们已进行了多次的熔融实验来确定的固相线温度诱导加热样品在活塞缸中的压力时间曲线变化。实验程序和材料实验进行装载用毫米的固体介质活塞圆筒装置(英寸)直径的NaCl石墨电池组件。测量和ptptrh热电偶连接到欧陆控制器控制温度。电子德鲁克PTX压力变送器测量机油压力连接到欧姆龙eck控制器。采用天然岩石样品和合成材料。毫克的细碎粉末(–毫米)被密封在一个黄金胶囊随后被嵌入在压力下的NaCl插头在室温下。由于固相线温度的确定主要依靠检测样品压实该技术只适用于缺乏流体实验。含水样品不合适因为水会在发生熔化填充多孔骨料。体积的影响减少由熔化的样品引起的压实可以放大以多孔骨料作为熔体的陷阱。我们使用的石英和钻石聚集在这两种情况下取得了良好的效果。与过量的石英岩样品(例如泥质岩和片麻岩)一个石英陷阱引入的熔融温度没有影响。二氧化硅可怜的组合物(例如斜长角闪岩)一个钻石陷阱使用更合适。由于样品的压实压力测量的变化通常是非常小的(小于条油压力)一般只持续很短的时间(小于秒)。检测由于融化在胶囊内的任何变化我们进行了多次实验应用热观察系统在很短的时间间隔响应小的增量。大会通过增加功率手动预定百分比的总功率每秒。我们选择这个时间间隔是因为它足以确保热平衡在装配之前下一个输入能量达到加热。用金刚石或石英陷阱的实验中压实可以慢因为熔体必须迁移通过多孔骨料。这些实验加热的增量是延长到秒期间的第一个秒加热后增斜坡产生温度和压力类似的斜坡。温度和压力是那么的平衡在接下来的功率增加。如果体积减少发生通过压力斜坡斜坡或转折变化表示的时间间隔内。加热的增量增加功率手动从温度控制器的感应。这个程序我们确保相同的能量增量用于每个时间间隔。能量的增加必须尽可能准确地确定熔化发生时的温度。能量的增加也必须足够大以产生大于测量误差的温度升高。我们估计在的电力供应增量足以产生约–C温度的升高。测量设备和数据记录检测P和T的小的变化在这些实验中产生的它是需要使用高精度的测量设备和记录的压力和温度不断。将所得的数据被用来构建PT和TT曲线。在我们的实验中温度控制和连续使用一个欧陆控制器监控有一个内部的冰点补偿器连接到计算机的数据采集和存储。该控制器具有手动模式我们使用所需的时间间隔内产生的温度升高。通过电子德鲁克PTX压力变送器测量活塞的RAM大门油压力并通过欧姆龙继电器eck控制器监视。该变送器的精度允许我们检测条油压力的变化(约巴在胶囊)。在欧姆龙继电器控制器还连接到计算机并测量压力的连续记录和实时显示。实验所用的材料在泥质片麻岩不同压力下测定了固相线温度和氯化锂。采用经典方法先前被确定为片麻岩固相线即检测存在或不存在的熔体在运行几天后的反应。这块岩石的矿物成分是约的石英毫秒转PL和个。对其组成和融化的关系在卡斯特罗等人给出的细节。。其固相线的石英KFSMS的存在故障的控制和PL氯化锂在温度低于氯化钠介质压力融化和氯化锂的固相线温度的立场是众所周知的(克拉克循环)。由于锂是在室温下压实钻石陷阱(例如广濑和钏路)在这些实验中使用。结论图显示了从熔融实验与泥质片麻岩进行曲线。在PT曲线趋势表现出不同的风格。压力下降发生在巴C。请注意PT曲线恢复初始斜率几秒钟后一旦熔体填充毛孔。第二期的结果是一个高原压力几乎是恒定的。这是在巴的片麻岩solidii确定的情况下C和巴C。高原发生在约秒的时间间隔来填补的熔体陷阱在这两个实验的孔隙的时间(DB和石英颗粒钻石)。三分之一结果的PT曲线斜率的变化。一个例子是在巴决定片麻岩固相线C。得到了用钻石陷阱氯化锂粉实验类似的结果。钻石陷阱填充慢慢产生的PT曲线的轻微变化。效果的在图d的PT曲线是斜率S形的拐点在巴C综述压力时间曲线的解释三个实验P,巴的泥质片麻岩产生相似的PT曲线进行。压力增加的速度比较慢在实验和熔点附近的速度开始。压力高原后(或压力下降)率降低到原来的值接近。这些波动是系统性的并反映在装配在加热过程中的力–bars在最初的学效应。例如在巴的实验压力升高率~秒和~–bars从那时直到达到高原。在高原在在秒的第一类似的结果观察在巴进行实验得到的速度接近压力增加。的温度时间曲线几乎恒定的斜率表明热平衡是在每个功率增量达到。然而这是没有压力的情况下。在PT曲线斜率的变化表明力学效应(扩张和变形)不是由组件完全吸收在每个时间间隔的功率增量。显然一些影响传播到随后的功率增加造成的PT曲线的斜率增加。这些累积的效应被完全吸收由装配在高原和压力的增加恢复的初始速率。我们的观点是这些系统的边坡的变化不是我们的实验文物相反它们是由于该组件的力学响应。显然通过时间间隔长机械效应可以通过该组件变形完全消退。然而结果并不完善因为主要目的是检测在高原的温度或压力降低在PT曲线观察。因此测得的压力在高原区间样品中真正的压力因此在该压力的样品融化。对于泥质片麻岩和氯化锂固相线为片麻岩和氯化锂的固相线的测定可以用来定位的固相线的曲线在PT空间。为OllodeSapo片麻岩曲线与以前的实验结果相比其固相线温度是通过经典的技术与扫描电镜观察抛光实验确定。在这个经典的技术的固相线温度测定的精度取决于必要的实验次数支架的熔点在一个狭窄的区间。以文中描述的测定是准确的~C在本研究中所用的实际固相线接近无熔点在巴和接近熔点在巴的泥质片麻岩增量加热技术。这里描述的技术更精确因为它依赖于由熔化的胶囊内开始引起的力学效应。基于对实验运行在近固相线的条件下观察熔体仅约体积的需要产生所观察到的力学效应。该技术还密切再现由克拉克氯化锂的固相线()(参见波伦)。这种材料的行为差别很大从硅酸盐。压实作用是在泥质片麻岩更容易检测。然而我们注意到通过应用技术的氯化锂熔炼得到的固相线点非常接近先前确定的固相线的曲线。参考文献波伦SR()精确压力校准平衡活塞缸装置和摩擦小炉装置。,Castro,A,PatiñoDouce,AE,Corretgé,LG,delaRosa,JD,ElBiad,M,andElHmidi,H()花岗岩和花岗闪长岩成因伊比利亚地块西班牙。花岗岩成因的实验测试。矿物学、岩石学贡献,。克拉克()公司对八碱金属卤化物熔点压力的影响。化学物理学报。Hirose,KandKushiro,I()在高压下干periodotites部分熔融的组合物的测定:从使用聚集体的钻石periodotites隔离。地球和行星科学通讯。PatiñoDouce,AEandBeard,JS()黑云母片麻岩和石英岩从到巴的脱水熔融。岩石学杂志–。PatiñoDouce,AEandBeard,JS()P的影响f(O)和MgFe比在合金脱水熔融模型。岩石学杂志。PatiñoDouce,AEandHarris,N()对喜马拉雅深熔作用的实验约束。岩石学杂志。Singh,JandJohannes,W()熔融英云脱水。第一部分:开始融–。化。矿物学、岩石学贡献Vielzeuf,DandClemens,JD()云母石英缺乏流体熔融:实验与模型。美国矿物–。Vielzeuf,DandMontel,JM()部分熔融的铝合金。第一部分:缺乏流体实验和相位关系。矿物学、岩石学贡献–。威利PJ()地壳深熔作用:实验观察。构造物理–。外文原文AnewmethodfordeterminingthefluidabsentsolidustemperatureinpistoncylinderexperimentsABSTRACTWedescribeanewpistoncylindermethodfordeterminingthefluidabsentsoliduscurvesofgeologicalmaterialsSamplesareheatedincrementallyatpressuresfromtokbarforperiodslessthanonehourTheeffectsofmeltingonthemeasuredoilpressurearesmallbutdetectableandyieldanaccuratesolidusbyinterpretationofpressuretimedataThetechniquesuccessfullyreproducesthesoliduscurveforLiClResultsfortheOllodeSapopeliticgneissaresuperiortothoseobtainedpreviouslyusingamoreconventionaltechniqueINTRODUCTIONTheidentificationofmagmasourcesintheEarth’smantleandcrustisfacilitatedbytheresultsofexperimentalpetrologyThePTpositionsofsoliduscurvesfordeepprotolithsarecriticaltounderstandingtheprocessesofmagmagenerationSoliduscurvesforpotentialcrustalsourcematerials,suchasamphibolitesandpelites,havebeendeterminedexperimentally(eg,WyllieSinghandJohannesPetöPatiñoDouceandBeard,PatiñoDouceandHarrisVielzeufandClemensVielzeufandMontel)Theseresultshaveshownthatvariationsinthemineralassemblages,orinthecompositionsofthemineralsolidsolutionsinvolvedinthemeltingreactions(eg,micaandplagioclase),canexertastronginfluenceonsolidustemperaturesConsequently,toproperlycharacterizemagmaproductionprocessesinaparticularenvironmentitisessentialtodeterminethesoliduscurvesforspecificcrustalprotolithsHowever,theworkisarduous,requiringmanytimeconsumingexperimentsinwhichthepresenceorabsenceofmeltisdeterminedbyobservationofscanningelectronmicroscope(SEM)imagesoftherunproductsThetechniquedescribedbelowcanbeusedtodeterminethepositionofasoliduscurveinPTspacebydirectobservationoftheeffectsofmeltingontheoilpressureinpistoncylinderapparatusTheseeffectsareverysmallbutcanbedetectedbyexaminationofapressuretime(Pt)curveproducedbyincrementalheatingRATIONALEWehavenoticedinpistoncylinderexperimentsthat–CvariationsintemperaturehaveameasurableeffectonpressureThisisobservedduringthefirstminutesofanexperimentwhentemperatureisrampedupwithatemperaturecontrollerAcorrespondingrampisobtainedwhenmeasuredpressureisplottedagainsttimeConsequently,compactionofthecapsulecontainerandorthesamplecapsulecanbedetectedbyvariationsinthemeasuredpressureduringheating,whichaffecttheslopeofthepressuretimecurveMeltingofthesamplewithinthecapsulewillproduceacompactioneffectthatmaybedetectedifpressureismeasuredveryaccuratelyanddataaretakencontinuouslyApplyingthismethod,wehaveconductedseveralmeltingexperimentstoidentifythesolidustemperaturebychangesinthepressuretimecurveinducedbyheatingofthesampleinthepistoncylinderEXPERIMENTALPROCEDURESANDSTARTINGMATERIALSExperimentswereperformedinendloaded,solidmediumpistoncylinderapparatuswithmm(inch)diameterNaClgraphitecellassembliesTemperaturesweremeasuredandcontrolledwithPtPtRhthermocoupleswiredtoEurothermcontrollersOilpressuresweremeasuredwithelectronicDRUCKPTXpressuretransmitters,connectedtoOMRONECKcontrollersWeusedbothnaturalrocksamplesandsyntheticmaterialsAboutmgoffinelycrushedpowder(–mm)weresealedwithinagoldcapsule,whichwassubsequentlyembeddedunderpressureinanNaClplugatroomtemperatureBecausedeterminationofthesolidustemperaturereliesondetectingsamplecompaction,thetechniqueonlyworksforfluidabsentexperimentsWaterbearingsamplesarenotappropriatebecausewaterwillfilltheporousaggregatebeforemeltingoccursTheeffectsofvolumereductionbymeltinginducedcompactionofthesamplecanbemagnifiedbyusingaporousaggregatethatactsasamelttrapWeusedquartzanddiamondaggregatesandobtainedgoodresultsinbothcasesForrocksampleswithexcessquartz(eg,pelitesandgneisses),theintroductionofaquartztraphadnoinfluenceonthemeltingtemperatureForsilicapoorcompositions(eg,amphibolites),theuseofadiamondtrapismoreappropriateMeasuredchangesinpressureduetocompactionofthesamplearenormallyverysmall(<baroilpressure),andgenerallylastonlyforashorttime(<s)Todetectanychangeduetomeltingwithinthecapsule,weperformedseveralexperimentsapplyingsmallincrementsofheatandobservingtheresponseofthesystemovershorttimeintervalsTheassemblywasheatedbyincreasingthepowermanuallyapredeterminedpercentageofthetotalpowereverysWechosethistimeintervalbecauseitissufficienttoensurethatthermalequilibriumwithintheassemblywasreachedbeforethenextenergyinput(Figa)Inexperimentsusingadiamondorquartztrap,compactionmaybeslowerbecausemeltmustmigratethroughtheporousaggregateForthoseexperimentsheatingincrementswerelengthenedtosDuringthefirstsafteraheatingincrement,arampisproducedfortemperature(Figb)andasimilarrampforpressure(Figc)TemperatureandpressurearethenrestabilizedbeforethenextpowerincreaseIfvolumereductionoccurswithinatimeintervalitisindicatedbyachangeintheslopeoraninflectioninthepressurerampsTheheatingincrementisinducedbyincreasingthepowermanuallyfromthetemperaturecontrollerWiththisprocedureweensurethatthesameenergyincrementisappliedforeachtimeinterval(Fig)TheenergyincrementmustbeassmallaspossibletodetermineaccuratelythetemperatureatwhichmeltingoccursTheenergyincreasemustalsobelargeenoughtoproducetemperatureincreasesthataregreaterthanmeasurementerrorWehaveestimatedthatanincrementinthepowersupplyofissufficienttoproduceatemperatureincreaseofabout–CMeasurementequipmentanddatarecordingTodetectthesmallchangesinPandTproducedintheseexperiments,itisnecessarytousehighprecisionmeasurementequipmentandtorecordpressuresandtemperaturescontinuouslyTheresultingdataareusedtoconstructPtandTtcurvesInourexperiments,temperaturewascontrolledandmonitoredcontinuouslyusinganEurothermcontroller,withaninternalicepointcompensator,connectedtoacomputerfordataacquisitionandstorageThecontrollerhasamanualmodethatweusedtoproducetemperatureincreaseswithinthedesiredtimeintervalsOilpressurewasmeasuredatthegateofthepistonrambyanelectronicDRUCKPTXpressuretransmitter,andmonitoredbyanONROMECKcontrollerTheprecisionofthistransmitterallowsustodetectvariationsofbaroilpressure(cabarinthecapsule)TheONROMcontrollerwasalsoconnectedtothecomputer,andmeasuredpressureswererecordedcontinuouslyanddisplayedinrealtimeMaterialsusedintheexperimentsSolidustemperaturesweredeterminedatdifferentpressuresforpeliticgneiss,andforLiClAsoliduscurveforthegneisswasdeterminedpreviouslyusingtheclassicalmethodthatis,detectingthepresenceorabsenceofmeltinrunsafterreactionforseveraldaysThemineralogicalcompositionofthisrockisapproximatelyQtz,Ms,Bt,Pl,andKfsDetailsonitscompositionandmeltingrelationsaregiveninCastroetal()ItssoliduscurveiscontrolledbythebreakdownofMsinthepresenceofQtz,Kfs,andPlLiClmeltsattemperatureslowerthanthatoftheNaClpressuremedium,andthePTpositionofthesoliduscurveforLiCliswellknown(ClarkBohlen)BecauseLiCliscompactedatroomtemperature,adiamondtrap(eg,HiroseandKushiro)wasusedintheseexperimentsRESULTSFigureshowsthecurvesobtainedfromthemeltingexperimentsperformedwiththepeliticgneissTrendsinthePtcurvesexhibitdistinctstylesApressuredecreaseoccurredatkbar,C(Figa)NotethatthePtcurveresumeditsinitialslopeafterseveralseconds,oncethemeltfilledtheporesAsecondPtresultisaplateauduringwhichpressureisnearlyconstantThisisthecaseforthegneisssolidiideterminedatkbar,C,andkbar,C(Figsbandd)Theplateauoccurredoveratimeintervalofabouts,thetimeneededtofilltheporesofthemelttrapusedinthesetwoexperiments(diamondsinbandquartzgrainsind)AthirdresultisachangeintheslopeofthePtcurveAnexampleisthegneisssolidusdeterminedatkbar,C(Figc)SimilarresultswereobtainedfortheexperimentswithLiClpowderusingadiamondtrap(Fig)ThediamondtrapfilledslowlyproducingslightchangesinthePtcurveTheeffectindicatedbythePtcurveinFiguredisasigmoidalinflectionintheslopeatkbar,CDISCUSSIONInterpretationofthepressuretimecurvesThethreeexperimentsperformedwiththepeliticgneissatP<kbarproducedsimilarPtcurvesTherateofpressureincreaseissloweratthebeginningoftheexperimentandfasternearthemeltingpointAfterthepressureplateau(orpressuredecrease),theratedecreasestoavalueclosetotheoriginaloneThesefluctuationsaresystematic,andreflectmechanicaleffectswithintheassemblyduringheatingForexample,intheexperimentperformedatkbar(Figb),therateofpressureincreasewas~–barsduringthefirsts,and~–barsfromthatpointuntiltheplateauwasreachedAftertheplateau,pressureincreasedatarateclosetothatobservedinthefirstsSimilarresultswereobtainedintheexperimentperformedatkbarThenearlyconstantslopeofthetemperaturetimecurvessuggeststhatthermalequilibriumwasreachedwithineachpowerincrementHowever,thisisnotthecaseforpressureThevariationsintheslopesofthePtcurvessuggestthatmechanicaleffects(dilatationanddeformation)arenotabsorbedcompletelybytheassemblywithineachtimeintervalofpowerincrementEvidently,someoftheeffectspropagatetothesubsequentpowerincrement,causingtheslopeofthePtcurvetoincreaseTheseaccumulatedeffectsareabsorbedcompletelybytheassemblyduringtheplateau,andpressureincreasesresumeattheinitialrateItisourviewthatthesesystematicslopechangesarenotartifactsofourexperimentsrather,theyareduetothemechanicalresponsesoftheassemblyClearly,bymakingthetimeintervalslonger,themechanicaleffectscouldbedissipatedcompletelybydeformationoftheassemblyHowever,resultswouldnotimprove,becausethemainaimistodetectthetemperatureatwhichaplateau,orpressuredecrease,isobservedinthePtcurveConsequently,themeasuredpressureduringtheplateauintervalistherealpressureinthesampleand,therefore,thepressureatwhichmeltingofthesampleoccurredSoliduscurvesforthepeliticgneissandLiClThePTsolidusdeterminationsforthegneissandLiClcanbeusedtolocatethesoliduscurvesinPTspace(Fig)ThecurvefortheOllodeSapogneissiscomparedwithpreviousexperimentalresults,inwhichthesolidustemperaturewasdeterminedbytheclassicaltechniqueobservingthepolishedexperimentalrunswithanSEMInthisclassicaltechniquetheaccuracyofthesolidustemperaturedeterminationdependsonthenumberofexperimentsnecessarytobracketthemeltingpointoveranarrowintervalWiththeincrementalheatingtechniquedescribedinthispaperthedeterminationisaccurateto~CInthepeliticgneissusedinthisstudytherealsoliduscurveisclosertothenomeltpointatkbarandclosertothemeltpointatkbar(Fig)ThetechniquedescribedhereismoreprecisebecauseitdependsonamechanicaleffectinducedbythebeginningofmeltingwithinthecapsuleBasedonobservationsoftheexperimentalrunsperformedatnearsolidusconditions,onlyaboutvolmeltisrequiredtoproducetheobservedmechanicaleffectsThetechniquealsocloselyreproducesthesoliduscurveforLiCldeterminedbyClark()(cfBohlen)ThebehaviorofthismaterialdiffersconsiderablyfromsilicatesThecompactioneffectsaredetectedmorereadilyinthepeliticgneissHowever,wenotethatthesoliduspointsobtainedbyapplyingthetechniquetoLiClmeltingareveryclosetothepreviouslydeterminedsoliduscurve(Fig)WeconcludethattheincrementalheatingtechniqueisanaccuratemethodformeasuringfluidabsentsolidiiThemethodpermitsthesolidusPTconditionsofanysilicaterocktobedeterminedbyperformingasingle,shortduration(h)pistoncylinderexperimentREFERENCESCITEDBohlen,SR()EquilibriaforprecisepressurecalibrationandafrictionlessfurnaceassemblyforthepistoncylinderapparatusNeuesJahrbuchfürMineralogieMonatshefte,,–Castro,A,PatiñoDouce,AE,Corretgé,LG,delaRosa,JD,ElBiad,M,andElHmidi,H()Originofperaluminousgranitesandgranodiorites,Iberianmassif,SpainAnexperimentaltestofgranitepetrogenesisContributionstoMineralogyandPetrology,,–Clark,SP()EffectofpressureonthemeltingpointofeightalkalihalidesJournalofChemicalPhysics,,–Hirose,KandKushiro,I()Partialmeltingofdryperiodotitesathighpressures:DeterminationofcompositionsofmeltssegregatedfromperiodotitesusingaggregatesofdiamondEarthandPl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