Designation: D 1308 – 87 (Reapproved 1998)
Standard Test Method for
Effect of Household Chemicals on Clear and Pigmented
Organic Finishes1
This standard is issued under the fixed designation D 1308; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope
1.1 This test method covers determination of the effect of
household chemicals on clear and pigmented organic finishes,
resulting in any objectionable alteration in the surface, such as
discoloration, change in gloss, blistering, softening, swelling,
loss of adhesion, or special phenomena.
1.2 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use.
2. Referenced Documents
2.1 ASTM Standards:
D 609 Practice for Preparation of Cold-Rolled Steel Panels
for Testing Paint, Varnish, Conversion Coatings, and
Related Coating Products2
3. Summary of Test Method
3.1 Three test methods, each of which is particularly appli-
cable to individual reagents under study, are described as
follows:
3.1.1 Spot Test, Covered—The reagent is placed on the test
surface and immediately covered with a watch glass.
3.1.2 Spot Test, Open—The test surface is subjected directly
to the effect of substance, such as citrus fruit, oils, greases,
beverages, etc.
3.1.3 Immersion Test—A suitably prepared panel is im-
mersed in the test reagent.
4. Significance and Use
4.1 Resistance to various liquids used in the home is an
important characteristic of organic finishes. These test methods
provide the means by which the relative performance of
coating systems may be evaluated. It should be recognized that
continuous films are necessary for reliable results.
5. Test Panels
5.1 Steel Panels—See Test Method D 609.
5.2 Other Metal Panels, as agreed upon by the purchaser
and the seller of the finish being tested.
6. Reagents
6.1 The choice of reagent shall be governed by ultimate
coating use and by agreement between the purchaser and the
seller of the finish being tested. The following reagents are
suggested:
6.1.1 Distilled Water, cold.
6.1.2 Distilled Water, hot.
6.1.3 Ethyl Alcohol (50 % volume).
6.1.4 Vinegar (3 % acetic acid).
6.1.5 Alkali Solution.
6.1.6 Acid Solution.
6.1.7 Soap Solution.
6.1.8 Detergent Solution.
6.1.9 Lighter Fluid and Other Volatile Reagents.
6.1.10 Fruit—Piece of cut fruit, with cut portion placed face
down on panel for time agreed upon between the purchaser and
the seller.
6.1.11 Oils and Fats—Butter, margarine, lard, shortening,
vegetable oils, etc.
6.1.12 Condiments—Mustard, catsup (ketchup).
6.1.13 Beverages—Coffee, tea, cocoa.
6.1.14 Lubricating Oils and Greases.
6.1.15 Other Reagents, as agreed upon between the pur-
chaser and the seller.
7. Procedure
7.1 Panel Preparation—Spot and direct application tests
may be carried out on the fabricated article coated with the
finishing system under evaluation, if sufficient plane surface is
available. For immersion tests and tests where the finished
article is not available, select panels in accordance with
Methods D 609, or prepare special metal panels according to
agreement between the purchaser and the seller of the finish.
Apply the finish according to the method and the schedule
prescribed by the user of the lacquer. This schedule includes
number of coats, film thickness, and other features. Allow the
finished panels to age 1 week at normal room conditions, about
1 This test method is under the jurisdiction of ASTM Committee D-1 on Paint
and Related Coatings, Materials, and Applications and is the direct responsibility of
Subcommittee D01.55 on Factory-Applied Coatings on Preformed Products.
Current edition approved May 29, 1987. Published July 1987. Originally
published as D 1308 – 54 T. Last previous edition D 1308 – 79 (1981)e1.
2 Annual Book of ASTM Standards, Vol 06.01.
1
AMERICAN SOCIETY FOR TESTING AND MATERIALS
100 Barr Harbor Dr., West Conshohocken, PA 19428
Reprinted from the Annual Book of ASTM Standards. Copyright ASTM
NOTICE:¬This¬standard¬has¬either¬been¬superseded¬and¬replaced¬by¬a¬new¬version¬or
discontinued.¬Contact¬ASTM¬International¬(www.astm.org)¬for¬the¬latest¬information.
77°F (25°C) and 50 % relative humidity, before testing.
7.2 Spot Test, Covered—Conduct the test at 73.5 6 3.5°F
(23 6 2°C) and 50 6 5 % relative humidity, or as agreed upon
between the purchaser and the seller. Using a 5-mL pipet
graduated in 0.1 mL, pipet onto the horizontal panel 1 mL of
the reagents listed in Section 6 and immediately cover with a
watch glass. After an interval agreed upon by the purchaser and
the seller, wipe the spot clean and examine immediately for
effects as listed in 1.1. Frequently used intervals are 15 min, 1
h, and 16 h, or by agreement between the producer and the
user. If desired, allow the panel to recover for a specified
period, and examine for return of original properties.
7.3 Spot Test, Open—Conduct the test at 73.5 6 3.5°F (23
6 2°C) and 50 6 5 % relative humidity, or as agreed upon
between the purchaser and the seller. Place a small portion of
the reagent on a horizontal panel or surface, with the exception
of fruit juices, as mentioned in 5.1.10. After a time interval, as
agreed upon between the purchaser and the seller, wipe the spot
clean and examine immediately for effects as listed in 1.1.
Frequently used intervals are 15 min, 1 h, and 16 h, or by
agreement between the producer and the user. If desired, allow
the panel to recover for a specified period and examine for
return of original properties.
7.4 Immersion—Immerse panels to a depth of 50 % in the
specified reagents (6.1.1, 6.1.2, 6.1.5, 6.1.6, 6.1.7, and 6.1.8)
contained in beakers, at a temperature and length of time
agreed upon between the purchaser and the seller. Withdraw
the panels, wash with distilled water, and examine immediately
for any of the effects listed in 1.1. If desired, allow the panels
to recover for a specified period and examine for return of the
original properties. In general, it will not be necessary to seal
the edges of the applied film. If the reagent effect is noted only
around the panel edges, the test should be repeated using a
suitable edge sealer. When sealing of edges is required, the
selection of the sealer should be a matter of agreement between
the purchaser and the seller.
8. Report
8.1 Report the following information:
8.1.1 System and the testing method employed. The test
conditions are an important factor in the results obtained and,
therefore, should be defined in the report.
8.1.2 The type of the effect, if any (see 1.1).
9. Precision and Bias
9.1 This test is designed to provide a working procedure for
examination of the effect of household chemicals on clear and
pigmented organic finishes. The effects will be in terms of
appearance, and numerical values are assigned if a rating scale
is used. Precision numbered values are not usually obtained for
this type of qualitative test.
10. Keywords
10.1 coating; metal; household chemicals; stain test
The American Society for Testing and Materials takes no position respecting the validity of any patent rights asserted in connection
with any item mentioned in this standard. Users of this standard are expressly advised that determination of the validity of any such
patent rights, and the risk of infringement of such rights, are entirely their own responsibility.
This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM Headquarters. Your comments will receive careful consideration at a meeting of the responsible
technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should make your
views known to the ASTM Committee on Standards, 100 Barr Harbor Drive, West Conshohocken, PA 19428.
D 1308
2
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