Agilent1100系列液质联用仪入门参考手册

� HP 1100 LC/MSD Gsbookl%.fm Page 1 Wednesday, November 1, 2000 1:52 PM — 2 — Help Help Topics Help Contents Index Find Display Close Print popup Print Cancel Help Topic Open Close I Open Help Contents Gsbookl%.fm Page 2 Wednesday, November 1, 2000 1:52 PM — 3 — View HP LC/MSD Reference CollectionCD ROM OQ/PV GLP EMF LC/MSD CD-ROM MSD LC/MSD Gsbookl%.fm Page 3 Wednesday, November 1, 2000 1:52 PM — 4 — LC/MSD DAD / Gsbookl%.fm Page 4 Wednesday, November 1, 2000 1:52 PM — 5 — FIA FIA : • FIA • Edit FIA Series. • Enable FIA Series in Method FIA . Single Sample Sequence Gsbookl%.fm Page 5 Wednesday, November 1, 2000 1:52 PM — 6 — DAD LC/MSD Integration Gsbookl%.fm Page 6 Wednesday, November 1, 2000 1:52 PM — 7 — UV MS Calibration . Signals Spectral Gsbookl%.fm Page 7 Wednesday, November 1, 2000 1:52 PM — 8 — : / MS Gsbookl%.fm Page 8 Wednesday, November 1, 2000 1:52 PM — 9 — x y Gsbookl%.fm Page 9 Wednesday, November 1, 2000 1:52 PM — 10 — † † † † † File/Add to Report Styles Gsbookl%.fm Page 10 Wednesday, November 1, 2000 1:52 PM — 11 — \hpchem\repstyle SIMPLE.FRP I NESTED.FRP SPECTRA.FRP PURITY.FRP ESTD.FRP AREAPCT.FRP LIBRARY.FRP Gsbookl%.fm Page 11 Wednesday, November 1, 2000 1:52 PM — 12 — OQ/PV / Gsbookl%.fm Page 12 Wednesday, November 1, 2000 1:52 PM — 13 — Verification View ShowTopToolbar . Verification (OQ/PV) • (OQ) • (PV) † VWD † † † † † DAD † * † † / * † * LC/MSD Gsbookl%.fm Page 13 Wednesday, November 1, 2000 1:52 PM — 14 — CD-ROM Gsbookl%.fm Page 14 Wednesday, November 1, 2000 1:52 PM — 15 — MSD MSD LC/MSD LC/MSD Gsbookl%.fm Page 15 Wednesday, November 1, 2000 1:52 PM — 16 — LC LC/MSD 1 Method and Run Control On 2 LC 3 LC/MSD 15 APCI LC/MSD 1 LC 50:50 / 5-10 2 Off LC/MSD 20psi 3L/min 300 APCI 325 MS LC to Waste(LC ) Gsbookl%.fm Page 16 Wednesday, November 1, 2000 1:52 PM — 17 — LC/MSD LC/MSD HPLC LC LC/MSD • • • LC/MSD LC/MSD .tun LC/MSD LC/MSD 4 4 LC/MSD LC/MSD 1 MSD Tune Tune/ Autotune Autotune 2 LC/MSD 1 Tune / Check Tune. 2 Check Tune • • (<150amu) • 4 1 (fragmentor skim2 1 2 2 3 4 fragmentor fragmentor Gsbookl%.fm Page 17 Wednesday, November 1, 2000 1:52 PM — 18 — LC/MSD • • • FIA • • • • Method and Run Control 1 Method / Load Method Open Method 2 Method / Edit Entire Method Help 3 ( ) 4 5 DAD VWD MSD MSD 6 7 Run Time Checklist( ) 8 Method / Save Method As Save Method 9 Start Gsbookl%.fm Page 18 Wednesday, November 1, 2000 1:52 PM — 19 — Deconvolution Deconvolution 1 Data Analysis MS 2 Spectral 3 Enter Deconvolution Tool 4 Find Ions 5 Î ÃFind Ions Options 6 Run Deconvolution ( Specra/ Deconvolution 7 Component ± £ 8 Preview Deconvolution Report Print Report 9 Compont List Delete Componts 4 10 Gaussian Gsbookl%.fm Page 19 Wednesday, November 1, 2000 1:52 PM — 20 — o o o o MS o HP 1100 Series LC/MSD Maintenance CD-ROM o Maintenance Logbook EMF o o o o o LC/MSD o ZDV T o SIM Ñ £ o (APCI) 1.0ml/min 0.5-1.5 ml/min ( ) SIM SIM Gsbookl%.fm Page 20 Wednesday, November 1, 2000 1:52 PM — 21 — † † † LC/MSD † LC/MSD † † fragmentor † † † † † LC/MSD † † † † † † LC † † † † † LC † >18M † LC † † † LC † † † † MS LC to MSD † Fragmentor † † Gsbookl%.fm Page 21 Wednesday, November 1, 2000 1:52 PM — 22 — HP 1100 LC LC DAD VWD) Gsbookl%.fm Page 22 Wednesday, November 1, 2000 1:52 PM — 23 — LC CAN HP-IB CAN Gsbookl%.fm Page 23 Wednesday, November 1, 2000 1:52 PM — 24 — HP 1100 LC/MSD On/off þ> LC Gsbookl%.fm Page 24 Wednesday, November 1, 2000 1:52 PM — 25 — HP 1100 LC/MSD APCI APCI On/off APCI APCI LC Gsbookl%.fm Page 25 Wednesday, November 1, 2000 1:52 PM — 26 — HP 1100 LC/MSD ( ) MS LC Gsbookl%.fm Page 26 Wednesday, November 1, 2000 1:52 PM — 27 — LC/MSD ( , ) LC/MSD HP-IB LC/MSD LC (N2) (N2) Gsbookl%.fm Page 27 Wednesday, November 1, 2000 1:52 PM — 28 — HP 1100 LC/MSD APCI ( ) MS APCI APCI LC Gsbookl%.fm Page 28 Wednesday, November 1, 2000 1:52 PM — 29 — LC/MSD APCI ( , ) LC/MSD HP-IB LC/MSD LC (N2) (N2) APCI APCI Gsbookl%.fm Page 29 Wednesday, November 1, 2000 1:52 PM — 30 — LC/MSD HP ES OQ/PV G1946-85001 G1946-85002 G1946-85006 G1946-85005 G1946-85004 G1946-85003 , F120 ( PEEK ) bal 1/4" PEEK 0.005", 1/16" G1946-80009 9301-1397 05971-80103 0100-1920 0100-1516 0905-1475 0101-0941 G1946-20177 G1946-20097 5182-3441 0890-1915 6040-0834 8660-0852 05980-60051 9300-1751 Gsbookl%.fm Page 30 Wednesday, November 1, 2000 1:52 PM — 31 — HP 1100 LC/ MSD HP 1100 LC/MSD IEC 1010 1 LC LC/MSD LC LC/MSD LC LC/MSD HP 1100 LC X Z H P LC/MSD LC/MSD LC/MSD Gsbookl%.fm Page 31 Wednesday, November 1, 2000 1:52 PM , 5/97 HP G2710 LC/MSD A.05.01 ©1997 . 5/97G1946-97006 � Gsbookl%.fm Page 32 Wednesday, November 1, 2000 1:52 PM