Designation: A 320/A 320M – 02 An American National Standard
Standard Specification for
Alloy/Steel Bolting Materials for Low-Temperature Service1
This standard is issued under the fixed designation A 320/A 320M; the number immediately following the designation indicates the year
of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval.
A superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope *
1.1 This specification2 covers alloy steel bolting materials
for pressure vessels, valves, flanges, and fittings for low-
temperature service. The term “bolting material” as used in this
specification covers rolled, forged, or strain hardened bars,
bolts, screws, studs, and stud bolts. The bars shall be hot-
wrought. The material may be further processed by centerless
grinding or by cold drawing. Austenitic stainless steel may be
solution annealed or annealed and strain-hardened. When
strain hardened austenitic stainless steel is ordered, the pur-
chaser should take special care to ensure that Appendix X1 is
thoroughly understood.
1.2 Several grades are covered, including both ferritic and
austenitic steels designated L7, B8, etc. Selection will depend
on design, service conditions, mechanical properties, and
low-temperature characteristics. The mechanical requirements
of Table 1 indicate the diameters for which the minimum
mechanical properties apply to the various grades and classes,
and Table 2 stipulates the requirements for Charpy impact
energy absorption. The manufacturer should determine that the
material can conform to these requirements before parts are
manufactured. For example, when Grade L43 is specified to
meet the Table 2 impact energy values at −150°F [−101°C],
additional restrictions (such as procuring a steel with lower P
and S contents than might normally be supplied) in the
chemical composition for AISI 4340 are likely to be required.
NOTE 1—The committee formulating this specification has included
several grades of material that have been rather extensively used for the
present purpose. Other compositions will be considered for inclusion by
the committee from time to time as the need becomes apparent. Users
should note that hardenability of some of the grades mentioned may
restrict the maximum size at which the required mechanical properties are
obtainable.
1.3 Nuts for use with this bolting material are covered in
Section 9 and the nut material shall be impact tested.
1.4 Supplementary Requirements (S1, S2, and S3) of an
optional nature are provided. They shall apply only when
specified in the inquiry, contract and order.
1.5 This specification is expressed in both inch-pound units
and in SI units. However, unless the order specifies the
applicable “M” specification designation (SI units), the mate-
rial shall be furnished to inch-pound units.
1.6 The values stated in either inch-pound units or SI units
are to be regarded separately as standard. Within the text, the
SI units are shown in brackets. The values stated in each
system are not exact equivalents; therefore, each system must
be used independently of the other. Combining values from the
two systems may result in nonconformance with the specifi-
cation.
2. Referenced Documents
2.1 ASTM Standards:
A 194/A 194M Specification for Carbon and Alloy Steel
Nuts for Bolts for High-Pressure or High-Temperature
Service, or Both3
A 370 Test Methods and Definitions for Mechanical Testing
of Steel Products4
A 962/A 962M Specification for Common Requirements
for Steel Fasteners or Fastener Materials, or Both, Intended
for Use at Any Temperature from Cryogenic to the Creep
Range3
E 566 Practice for Electromagnetic (Eddy-Current) Sorting
of Ferrous Metals5
F 436 Specification for Hardened Steel Washers6
2.2 ANSI Standards:
B1.1 Screw Threads7
B18.22.1 Plain Washers7
3. Ordering Information
3.1 It is the purchaser’s responsibility to specify in the
purchase order all information necessary to purchase the
needed materials. Examples of such information include, but
1 This specification is under the jurisdiction of ASTM Committee A01 on Steel,
Stainless Steel, and Related Alloys and is the direct responsibility of Subcommittee
A01.22 on Steel Forgings and Wrought Fittings for Piping Applications and Bolting
Materials for Piping and Special Purpose Applications.
Current edition approved March 10, 2002. Published May 2002. Originally
published as A 320 – 48 T. Last previous edition A 320/A 320M – 01.
2 For ASME Boiler and Pressure Vessel Code applications, see related Specifi-
cation SA-320 in Section II of that Code.
3 Annual Book of ASTM Standards, Vol 01.01.
4 Annual Book of ASTM Standards, Vol 01.03.
5 Annual Book of ASTM Standards, Vol 03.03.
6 Annual Book of ASTM Standards, Vol 01.08.
7 Available from American National Standards Institute, 11 West 42nd St., 13th
Floor, New York, NY 10036.
1
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
are not limited to, the following:
3.1.1 Quantity and size,
3.1.2 Heat-treated condition, that is, for the austenitic stain-
less steels, solution-treated (Class 1); solution-treated after
finishing (Class 1A); and annealed and strain-hardened (Class
2),
3.1.3 Description of items required (bars, bolts, screws, or
studs),
3.1.4 Nuts and washers, if required by the purchaser, in
accordance with Section 9, and
3.1.5 Special requirements, in accordance with 5.1.1, 5.1.2,
5.1.3, and 11.1.
4. Common Requirements
4.1 Material and fasteners supplied to this specification shall
conform to the requirements of Specification A 962/A 962M.
These requirements include methods, finish, thread dimen-
sions, marking certification, optional supplementary require-
ments, and others. Failure to comply with the requirements of
Specification A 962/A 962M constitutes nonconformance with
this specification. In case of conflict between the requirements
in this specification and Specification A 962/A 962M, this
specification shall prevail.
4.2 For L7M bolting, the final heat treatment, which may be
TABLE 1 Mechanical Requirements
Class and Grade, Diameter, in [mm] Heat Treatment
Tensile
Strength,
min, ksi
[MPa]
Yield Strength,
min, ksi
[MPa] (0.2 %
offset)
Elongation
in 2 in.
or 50
mm min, %
Reduction
of Area,
min, %
Hardness
max
Ferritic Steels
L7, L7A, L7B, L7C, L70, L71, L72, L73 125 105 16 50 . . .
21⁄2 [65] and underA quenched and tempered [860] [725]
L43 125 105 16 50 . . .
4 [100] and underA quenched and tempered [860] [725]
L7M 100 80 18 50 235 HBB or
99 HRB
21⁄2 [65] and underA quenched and tempered at 1150°F
[620°C], min
[690] [550]
L1 125 105 16 50 . . .
1 [25] and underA quenched and tempered [860] [725]
Austenitic SteelsC
Class 1: B8, B8C, B8M, B8P,
B8F, B8T, B8LN, B8MLN, all diameters
carbide solution treated 75
[515]
30
[205]
30 50 223 HBD or
96 HRB
Class 1A: B8A, B8CA, B8MA, B8PA,
B8FA, B8TA, B8LNA,
B8MLNA, all diameters
carbide solution treated in the
finished condition
75
[515]
30
[205]
30 50 192 HB or 90
HRB
Class 2: B8, B8C, B8P, B8F, B8T: carbide solution treated and strain
hardened
3⁄4 [20] and under 125
[860]
100
[690]
12 35 321 HB or 35
HRC
over 3⁄4 to 1 [20 to 25], incl 115
[795]
80
[550]
15 30 321 HB or 35
HRC
over 1 to 11⁄4 [25 to 32], incl 105
[725]
65
[450]
20 35 321 HB or 35
HRC
over 11⁄4 to 11⁄2 [32 to 40], inclA 100
[690]
50
[345]
28 45 321 HB or 35
HRC
Class 2: B8M: carbide solution treated and strain
hardened
3⁄4 [20] and under 110
[760]
95
[655]
15 45 321 HB or 35
HRC
over 3⁄4 to 1 [20 to 25], incl 100
[690]
80
[550]
20 45 321 HB or 35
HRC
over 1 to 11⁄4 [25 to 32], incl 95
[655]
65
[450]
25 45 321 HB or 35
HRC
over 11⁄4 to 11⁄2 [32 to 40], inclA 90
[620]
50
[345]
30 45 321 HB or 35
HRC
A These upper diameter limits were established on the basis that these were the largest sizes commonly available that consistently met specification property limits. They
are not intended as absolute limits beyond which bolting materials could no longer be certified to the specification.
B To meet the tensile requirements, the Brinell hardness shall not be less than 200 HB or 93 HRB.
C Class 1 products are made from solution-treated material. Class 1A products are solution treated in the finished condition for corrosion resistance; heat treatment is
critical for enhancing this physical property and meeting the mechanical property requirements. Class 2 products are made from solution-treated material that has been
strain hardened. Austenitic steels in the strain-hardened condition may not show uniform properties throughout the cross section, particularly in sizes over 3⁄4in. [20 mm]
in diameter.
D For sizes 3⁄4 in. [20 mm] in diameter and smaller, a maximum hardness of 241 HB (100 HRB) is permitted.
TABLE 2 Impact Energy Absorption Requirements
Size of
Specimen, mm
Minimum Impact Value
Required for Average
of Each Set of Three
Specimens, ft·lbf [J]
Minimum Impact
Value Permitted for
One Specimen Only
of a Set, ft·lbf [J]
All Grades Except L1A
10 by 10
10 by 7.5
20 [27]
16 [22]
15 [20]
12 [16]
Grade L1
10 by 10
10 by 7.5
40 [54]
32 [44]
30 [41]
24 [32]
A See 6.2.1.1 for permitted exemptions.
A 320/A 320M
2
the tempering operation if conducted at 1150°F [620°C]
minimum, shall be done after machining and forming opera-
tions, including thread rolling and any type of cutting.
5. Materials and Manufacture
5.1 Heat Treatment:
5.1.1 The bolting material shall be allowed to cool to room
temperature after rolling or forging. Grades L7, L7A, L7B,
L7C, L7M, L43, L1, L70, L71, L72, and L73 shall be reheated
to above the upper critical temperature and liquid quenched
and tempered. Grades B8, B8C, B8M, B8T, B8F, B8P, B8LN,
and B8MLN shall receive a carbide solution treatment. Prod-
ucts made from such material are described as Class 1. This
shall consist of holding the material for a sufficient time at a
temperature at which the chromium carbide will go into
solution and then cooling in air or in a liquid medium at a rate
sufficient to prevent reprecipitation of the carbide. Material
thus treated is described as Class 1. If specified in the purchase
order, material shall be solution treated in the finished condi-
tion; material so treated is described as Class 1A.
5.1.2 When increased mechanical properties are desired, the
austenitic bolting materials shall be solution annealed and
strain hardened if specified in the purchase order; material so
treated is identified as Class 2.
5.1.3 If scale-free bright finish is required, this shall be
specified in the purchase order.
5.1.4 For L7M bolting, the final heat treatment, which may
be the tempering or stress-relieving operation conducted at
1150°F [620°C] minimum, shall be done after machining or
rolling of the threads.
6. Mechanical Requirements
6.1 Tensile Properties:
6.1.1 The material shall conform to the requirements as to
tensile properties prescribed in Table 1 at room temperature
after heat treatment (see 5.1.1).
6.1.2 Number of Tests:
6.1.2.1 For heat-treated bars, one tension test and one
impact test consisting of three specimens shall be made for
each diameter of each heat represented in each tempering
charge. In the continuous type treatment, a charge shall be
defined as 6000 lb [2700 kg].
6.1.2.2 For studs, bolts, screws, etc., one tension test and
one set of three impact specimens shall be made for each
diameter of each heat involved in the lot. Each lot shall consist
of the following:
Diameter, in. [mm] Lot Size, lb [kg]
11⁄8 [30] and under 1500 [680] or fraction thereof
Over 11⁄8 [30] to 13⁄4 [45],
incl
4500 [2040] or fraction
thereof
Over 13⁄4 [45] to 21⁄2 [65],
incl
6000 [2700] or fraction
thereof
Over 21⁄2 [65] 100 pieces or fraction thereof
6.1.2.3 Full Size Specimens, Headed Fasteners—Headed
fasteners 1 1⁄2 in. in body diameter and smaller, with body
length three times the diameter or longer, and which are
produced by upsetting or forging (hot or cold) shall be
subjected to full size testing in accordance with 6.1.3. This
testing shall be in addition to tensile testing as specified in
6.1.1. The lot size shall be shown in 6.1.2.2. Failure shall occur
in the body or threaded sections with no failure, or indications
of failure, such as cracks, at the junction of the head and shank.
6.1.3 Full Size Fasteners, Wedge Tensile Testing—When
applicable, see 6.1.2.3. Headed fasteners shall be wedge tested
full size in accordance with Annex A3 of Test Methods and
Definitions A 370 and shall conform to the tensile strength
shown in Table 1. The minimum full size breaking strength
(lbf) for individual sizes shall be as follows:
Ts 5 UTS 3 As (1)
where:
Ts = Wedge tensile strength
UTS = Tensile strength specified in Table 1, and
As = Stress area, square inches, as shown in ANSI B1.1
or calculated as follows:
As 5 0.785 ~D2~0.974/n!!2 (2)
where:
D = Nominal thread size, and
n = The number of threads per inch.
6.2 Impact Properties:
6.2.1 Requirements:
6.2.1.1 Material of Grades L7, L7A, L7B, L7C, L7M, L43,
L70, L71, L72, and L73 shall show a minimum impact energy
absorption of 20 ft · lbf [27 J] and of Grade L1 a minimum
impact energy absorption of 40 ft · lbf [54 J] at the test
temperature when tested by the procedure specified in the
applicable portions of Sections 19 to 28 of Test Methods and
Definitions A 370. The temperature of the coolant used for
chilling the test specimens shall be controlled within6 3°F
[1.5°C]. Impact tests are not required for carbide solution
treated or strain hardened Grades B8, B8F, B8P, B8M, B8T,
B8LN, and B8MLN for temperatures above −325°F [−200°C];
for carbide solution treated Grades B8, B8P, B8C, and B8LN
above −425°F [−255°C]; for all ferritic and austenitic steel
grades of bolting 1⁄2 in. [12.5 mm] and smaller in diameter. All
other material furnished under this specification shall be tested.
Test temperatures for ferritic grades are listed in Table 3.
Exceptions to this requirement are permissible, and the impact
tests may be made at specified temperatures different than
those shown in Table 3, provided the test temperature is at least
as low as the intended service temperature and the bolting is
suitably marked to identify the reported test temperature. When
impact testing is required for austenitic grades, test criteria
shall be agreed upon between the supplier and purchaser.
6.2.1.2 The impact test requirements for standard and sub-
size Charpy test specimens are prescribed in Table 2.
6.2.2 Number of Tests:
6.2.2.1 The test requirements for heat-treated bars are given
in 6.1.2.1.
TABLE 3 Recommended Test Temperature for Stock Parts
Grade
Test Temperature
°F °C
L7M, L70, L71, L72, L73 −100 −73
L7, L7A, L7B, L7C −150 −101
L43 −150 −101
L1 −100 −73
A 320/A 320M
3
6.2.2.2 For test requirements on studs, bolts, screws, etc.,
see 6.1.2.2.
6.2.2.3 Impact tests are not required to be made on heat-
treated bars, bolts, screws, studs, and stud bolts 1⁄2 in. [12.5
mm] and under in diameter.
6.2.3 Test Specimens—For sections 1 in. [25 mm] or less in
diameter, test specimens shall be taken at the axis; for sections
over 1 in. [25 mm] in diameter, midway between the axis and
the surface.
6.3 Hardness Requirements:
6.3.1 The hardness shall conform to the requirements pre-
scribed in Table 1.
6.3.2 The maximum hardness of Grade L7M shall be 235
HB or 99 HRB (conversion in accordance with Table Number
2B of Test Methods and Definitions A 370). Minimum hard-
ness shall not be less than 200 HB or 93 HRB.
6.3.2.1 The use of 100 % electromagnetic testing for hard-
ness as an alternative to 100 % indentation hardness testing is
permissible when qualified by sampling using indentation
hardness testing. Each lot tested for hardness electromagneti-
cally shall be 100 % examined in accordance with Practice
E 566. Following electromagnetic testing for hardness, a ran-
dom sample of a minimum of 100 pieces in each purchase lot
(as defined in 6.1.2.2) shall be tested by indentation hardness
methods. All samples must meet hardness requirements to
permit acceptance of the lot. If any one sample is outside of the
specified maximum or minimum hardness, the lot shall be
rejected and either reprocessed and resampled, or tested 100 %
by indentation hardness methods.
6.3.2.2 In the event a controversy exists relative to mini-
mum strength, tension tests shall prevail over hardness read-
ings. Products which have been tested and found acceptable
shall have a line under the grade symbol.
7. Workmanship, Finish, and Appearance
7.1 Bolts, screws, studs, and stud bolts shall be pointed and
shall have a workmanlike finish.
8. Retests
8.1 If the results of the mechanical tests of any test lot do
not conform to the requirements specified, the manufacturer
may retreat such lot not more than twice, in which case two
additional tension tests and one additional impact test consist-
ing of three specimens shall be made from such lot, all of
which shall conform to the requirements specified.
9. Nuts and Washers
9.1 Bolts, studs, and stud bolts of Grades L7, L7A, L7B,
L7C, L43, L1, L70, L71, L72, and L73 shall be equipped with
ferritic alloy nuts conforming to Grade 4 or Grade 7 of
Specification A 194/A 194M or a grade of steel similar to the
studs. Grade 7M nuts at a hardness not exceeding 235 HB (or
equivalent) shall be used with Grade L7M bolts, studs, and stud
bolts. All nut materials, including those which may be supplied
under Specification A 194/A 194M, shall be subject to the
impact requirements of this specification in the following
manner: impact tests shall be made on test specimens taken
from the bar or plate from the heat of steel used for manufac-
turing the nuts, and heat treated with the nut blanks.
9.2 Bolts, studs, and stud bolts of Grades B8, B8C, B8T,
B8P, B8F, B8M, B8LN, and B8MLN shall be equipped with
austenitic alloy nuts conforming to Grades 8, 8C, 8T, 8F, 8M,
8LN, and 8MLN for Specification A 194/A 194M. Impact tests
are not required for Grades 8F, 8M, 8T, and 8MLN for
temperatures above −325°F [−200°C] and for Grades 8, 8P, 8C,
and 8LN above −425°F [−255°C].
9.3 If the purchaser requires nuts with a Charpy impact
energy absorption of not less than 20 ft · lbf [27 J] at
temperatures below −150°F [−100°C], he may require that the
nuts conform to Grades 8, 8C, 8M, 8P, 8T, 8F, 8LN, or 8MLN
of Specification A 194/A 194M.
9.4 Washers for use with ferritic steel bolting shall conform
to Specification F 436.
9.5 Washers for use with austenitic steel bolting shall be
made of austenitic steel as agreed upon between the manufac-
turer and purchaser.
9.6 Washer dimensions shall be in accordance with require-
ments of ANSI B18.22.1, unless otherwise specified in the
purchase order.
10. Threads
10.1 Where practical, all threads shall be formed after heat
treatment. Class 1A, Grades B8A, B8CA, B8MA, B8PA,
B8FA, B8TA, B8LNA, and B8MLNA are to be solution-
treated in the finished condition.
11. Product Marking
11.1 The identification symbol shall be as shown in Table 4.
In the case of Class 2, Grades B8, B8C, B8M, B8P, B8F, and
B8T strain hardened as provided in Table 1, a line shall be
stamped under the grade symbol in order to distinguish it from
Class 1 and Class 1A bolting which has not been strain
hardened. In the case of Class 1A, the marking B8A, B8CA,
B8MA, B8PA, B8FA, B8TA, B8LNA, and B8MLNA identifies
the material as being in the solution-treated condition in the
finished state. Grade L7M which has been 100 % evaluated in
conformance with this specification shall have a line under the
grade symbol to distinguish it from L7M produced to previous
revisions not requiring 100 % hardness te
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